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Some Photoshop version like CS2 does not allow to Split Channels unless the CMYK image mode is converted to Multichannel first. If that is the case do the following:

1) Convert the image mode to CMYK
2) Convert the image mode to Multichannel
3) Click the Channels tab option button
4) Click Split Channels
5) Save each channel to desired file format.

Each channel will be grayscale. If they are not labeled with Cyan, Magenta, Yellow and black in the document names the order is as follows Channel 1 is Cyan, Channel 2 is Magenta, channel 3 is yellow and channel 4 is Black.
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